Lovibond 00386455 - MD1x0/200 - Manganese HR PP, Manganese LR PP, Manganese T Manuale utente

Tipo
Manuale utente
Lovibond® Water Testing
Tintometer® Group
Manual of Methods
MD 100 • MD 110 • MD 200
Manganese
EN
Manual of Methods
Page 4
DE
Methodenhandbuch
Seite 20
ES
Manual de Métodos
Página 36
FR
Méthodes Manuel
Page 52
IT
Manuale dei Metodi
Pagina 68
PT
Métodos Manual
Página 84
NL
Handboek Methoden
Zijde 100
ZH
方法手册
Page 116
NL Handboek van Methoden 01/20EN Handbook of Methods 01/20
KS4.3 T
0.1 - 4 mmol/l KS4.3
Acid / Indicator
20
S:4.3
Instrument specific information
The test can be performed on the following devices. In addition, the required cuvette
and the absorption range of the photometer are indicated.
Instrument Type Cuvette λMeasuring Range
MD 200, MD 600, MD 610,
MD 640, MultiDirect, PM 620,
PM 630
ø 24 mm 610 nm 0.1 - 4 mmol/l KS4.3
SpectroDirect, XD 7000,
XD 7500
ø 24 mm 615 nm 0.1 - 4 mmol/l KS4.3
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
Alka-M-Photometer Tablet / 100 513210BT
Alka-M-Photometer Tablet / 250 513211BT
Application List
Waste Water Treatment
Drinking Water Treatment
Raw Water Treatment
Notes
1. The terms Alkalinity-m, m-Value, total alkalinity and Acid demand to KS4.3 are iden-
tical.
2. For accurate results, exactly 10 ml of water sample must be used for the test.
Display in the MD
100 / MD 110 /
MD 200
Bar code for the
detection of the
methods
Method name
Measuring range
Chemical Method
Method number
Language codes
ISO 639-1 Revision status
KS4.3 T / 20
How to use
ENMethod Reference Book4
EN
Implementation of the provision Acid capacity KS4.3 with Tablet
Select the method on the device
For this method, no ZERO measurements are to be carried out with the following de-
vices: XD 7000, XD 7500
10 ml
Fill 24 mm vial with 10 ml
sample.
Close vial(s).
Sample
Place sample vial in the
sample chamber. • Pay
attention to the positioning.
Dissolve tablet(s) by inver-
ting.
Sample
Place sample vial in the
sample chamber. • Pay
attention to the positioning.
Test
Press the TEST (XD:
START) button.
The result in Acid Capacity KS4.3 appears on the display.
Performing test
procedure
KS4.3 T / 20
NL Handboek van Methoden 01/20EN Handbook of Methods 01/20
How to use
ENMethod Reference Book 5
EN
Manganese T / M240
ENMethod Reference Book1.06
EN
Manganese T M240
0.2 - 4 mg/L Mn Mn
Formaldoxime
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
Manganese LR 1 Tablet / 100 516080BT
Manganese LR 1 Tablet / 250 516081BT
Manganese LR 2 Tablet / 100 516090BT
Manganese LR 2 Tablet / 250 516091BT
Set Manganese LR 1/LR 2 100 Pc.#100 each 517621BT
Set Manganese LR 1/LR 2 250 Pc.#250 each 517622BT
Manganese T / M240
ENMethod Reference Book1.0 7
EN
Determination of Manganese with Tablet
Select the method on the device.
10 mL
Sample
Fill 24 mm vial with 10 mL
sample.
Close vial(s). Place sample vial in the
sample chamber. Pay
attention to the positioning.
Zero
Press the ZERO button. Remove the vial from the
sample chamber.
24 mm
Add MANGANESE LR
1 tablet .
Crush tablet(s) by rotating
slightly and dissolve.
Add MANGANESE LR
2 tablet .
Manganese T / M240
ENMethod Reference Book1.08
EN
24 mm
Crush tablet(s) by rotating
slightly.
Close vial(s). Dissolve tablet(s) by
inverting.
Sample
Test
9
4
5
6
7
8
10
11 12
1
2
3
5 min
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Press the TEST (XD:
START)button.
Wait for 5 minute(s)
reaction time.
Once the reaction period is finished, the measurement takes place automatically.
The result in mg/L Manganese appears on the display.
Manganese T / M240
ENMethod Reference Book1.0 9
EN
Analyses
The following table identifies the output values can be converted into other citation
forms.
Unit Cite form Scale Factor
mg/l Mn 1
mg/l MnO42.17
mg/l KMnO42.88
Chemical Method
Formaldoxime
Appendix
Bibliography
Gottlieb, A. & Hecht, F. Mikrochim Acta (1950) 35: 337
According to
DIN 38406-E2
# including stirring rod, 10 cm
Manganese LR PP / M242
ENMethod Reference Book1.010
EN
Manganese LR PP M242
0.01 - 0.7 mg/L Mn Mn1
PAN
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
VARIO Manganese Reagent, Set Low Range
F10
1 Pieces 535090
Vario Rochelle Salt Solution, 30 ml h) 30 mL 530640
Preparation
1. All lab glassware must first be rinsed with diluted nitric acid and then rinsed with
deionised water.
2. Strongly buffered water samples or extreme pH values may exceed the buffering
capacity of the reagents and pH values to be adjusted.
If samples were acidified for storing, the pH value must be adjusted between 4 and
5 with 5 mol/l (5 N) Sodium hydroxide before the test. A pH value of 5 must not be
exceeded, since this can lead to precipitation of manganese.
Remarks
1. If water samples contain more than 300 mg/L CaCO3 hardness, then after adding
the Vario Ascorbic Acid powder pack, add an additional 10 drops of Rochelle Salt
Solution.
2. After addition of the reagent solution “Alkaline-Cyanide” a cloudy or turbid solution
may form in some water samples. Adding the PAN indicator solution should resolve
the turbidity.
3. If the sample contains large amounts of iron (from 5 mg/L) a reaction period of 10
minutes must be adhered to.
Manganese LR PP / M242
ENMethod Reference Book1.0 11
EN
Determination of Manganese LR with Vario Powder Packs
Select the method on the device.
Blank
Blank
10 mL
Sample
10 mL
Prepare two clean 24 mm
vials. Mark one as a blank.
Put 10 mL deionised
water in the blank.
Put 10 mL sample in the
sample vial.
SampleBlank
Add a Vario Ascorbic
Acid powder pack in each
vial.
Close vial(s). Invert several times to mix
the contents.
15
Hold cuvettes vertically
and add equal drops by
pressing slowly.
Add 15 drops Alkaline-
Cyanide Reagenz.
Close vial(s).
Manganese LR PP / M242
ENMethod Reference Book1.012
EN
21
Invert several times to mix
the contents.
Add 21 drops PAN
Indikator.
Close vial(s).
9
4
5
6
7
8
10
11 12
1
2
3
2 min
Invert several times to mix
the contents.
Press the ENTER button. Wait for 2 minute(s)
reaction time.
Blank
Zero
Place blank in the sample
chamber. Pay attention to
the positioning.
Press the ZERO button. Remove the vial from the
sample chamber.
Manganese LR PP / M242
ENMethod Reference Book1.0 13
EN
Sample
Test
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Press the TEST (XD:
START)button.
The result in mg/L Manganese appears on the display.
Manganese LR PP / M242
ENMethod Reference Book1.014
EN
Analyses
The following table identifies the output values can be converted into other citation forms.
Unit Cite form Scale Factor
mg/l Mn 1
mg/l MnO42.17
mg/l KMnO42.88
Chemical Method
PAN
Appendix
Bibliography
Goto, K., et al., Talanta, 24, 652-3 (1977)
h) additionally required for samples with hardness values above 300 mg/l CaCO3
Manganese HR PP / M243
ENMethod Reference Book1.016
EN
Manganese HR PP M243
0.1 - 18 mg/L Mn Mn2
Periodate Oxidation
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
VARIO Manganese HR, Set High Range F10 1 Set 535100
Preparation
1. Strongly buffered water samples or extreme pH values may exceed the buffering
capacity of the reagents and pH values to be adjusted.
If samples were acidified for storing, the pH value must be adjusted between 4 and
5 with 5 mol/l (5 N) Sodium hydroxide before the test. A pH value of 5 must not be
exceeded, since this can lead to precipitation of manganese.
Manganese HR PP / M243
ENMethod Reference Book1.0 17
EN
Determination of Manganese HR with Vario Powder Packs
Select the method on the device.
10 mL
Sample
Fill 24 mm vial with 10 mL
sample.
Close vial(s). Place sample vial in the
sample chamber. Pay
attention to the positioning.
Zero
Press the ZERO button. Remove the vial from the
sample chamber.
Sample
Add Vario Manganese
Citrate Buffer F10 powder
pack.
Close vial(s). Mix the contents by shaking.
Manganese HR PP / M243
ENMethod Reference Book1.018
EN
Sample
Add Vario Sodium
Periodate F10 powder
pack.
Close vial(s). Mix the contents by shaking.
Sample
Test
9
4
5
6
7
8
10
11 12
1
2
3
2 min
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Press the TEST (XD:
START)button.
Wait for 2 minute(s)
reaction time.
Once the reaction period is finished, the measurement takes place automatically.
The result in mg/L Manganese appears on the display.
Manganese HR PP / M243
ENMethod Reference Book1.0 19
EN
Analyses
The following table identifies the output values can be converted into other citation
forms.
Unit Cite form Scale Factor
mg/l Mn 1
mg/l MnO42.17
mg/l KMnO42.88
Chemical Method
Periodate Oxidation
Appendix
Interferences
Interference from / [mg/L]
Ca 700
Cl-70000
Fe 5
Mg 100000
Method Validation
Limit of Detection 0.16 mg/L
Limit of Quantification 0.49 mg/L
End of Measuring Range 18 mg/L
Sensitivity 13.02 mg/L / Abs
Confidence Intervall 0.28 mg/L
Standard Deviation 0.12 mg/L
Variation Coefficient 1.29 %
According to
40 CFR 136 (US EPA approved HACH)
DE Methodenhandbuch 01/20
KS4.3 T
0,1 - 4 mmol/l KS4.3
Säure / Indikator
20
S:4.3
Instrumentspezifische Informationen
Der Test kann auf den folgenden Geräten durchgeführt werden. Zusätzlich sind die
benötigte Küvette und der Absorptionsbereich der Photometer angegeben.
Geräte Küvette λMessbereich
MD 200, MD 600, MD 610,
MD 640, MultiDirect, PM 620,
PM 630
ø 24 mm 610 nm 0,1 - 4 mmol/l KS4.3
SpectroDirect, XD 7000,
XD 7500
ø 24 mm 615 nm 0,1 - 4 mmol/l KS4.3
Material
Benötigtes Material (zum Teil optional):
Reagenzien Form/Menge Bestell-Nr.
Alka-M-Photometer Tablette / 100 513210BT
Alka-M-Photometer Tablette / 250 513211BT
Anwendungsbereich
Abwasserbehandlung
Trinkwasseraufbereitung
Rohwasserbehandlung
Anmerkungen
1. Die Begrie Alkalität-m, m-Wert, Gesamtalkalität und Säurekapazität KS4.3 sind
identisch.
2. Die exakte Einhaltung des Probevolumens von 10 ml ist für die Genauigkeit des
Analysenergebnisses entscheidend.
Displayanzeige
im MD 100 MD 110
/ MD 200
Barcode zur
Methodenerkennung
Methoden Name
Messbereich
Chemische
Methode
Methodennummer
Sprachkürzel nach
ISO 639-1 Revisionsstand
KS4.3 T / 20
Leitfaden für den Anwender
ENMethod Reference Book20
DE
Durchführung der Bestimmung Säurekapazität KS4.3 mit Tablette
Die Methode im Gerät auswählen.
Für diese Methode muss bei folgenden Geräten keine ZERO-Messung durchgeführt
werden: XD 7000, XD 7500
10 ml
24-mm-Küvette mit 10 ml
Probe füllen.
Küvette(n) verschließen.
Sample
Die Probenküvette in
den Messschacht stellen.
Positionierung beachten.
Tablette(n) durch Um-
schwenken lösen.
Sample
Die Probenküvette in
den Messschacht stellen.
Positionierung beachten.
Test
Taste TEST (XD: START)
drücken.
In der Anzeige erscheint das Ergebnis als Säurekapazität KS4.3.
Durchführung der
Messung
KS4.3 T / 20
DE Methodenhandbuch 01/20
Leitfaden für den Anwender
ENMethod Reference Book 21
DE
  • Page 1 1
  • Page 2 2
  • Page 3 3
  • Page 4 4
  • Page 5 5
  • Page 6 6
  • Page 7 7
  • Page 8 8
  • Page 9 9
  • Page 10 10
  • Page 11 11
  • Page 12 12
  • Page 13 13
  • Page 14 14
  • Page 15 15
  • Page 16 16
  • Page 17 17
  • Page 18 18
  • Page 19 19
  • Page 20 20
  • Page 21 21
  • Page 22 22
  • Page 23 23
  • Page 24 24
  • Page 25 25
  • Page 26 26
  • Page 27 27
  • Page 28 28
  • Page 29 29
  • Page 30 30
  • Page 31 31
  • Page 32 32
  • Page 33 33
  • Page 34 34
  • Page 35 35
  • Page 36 36
  • Page 37 37
  • Page 38 38
  • Page 39 39
  • Page 40 40
  • Page 41 41
  • Page 42 42
  • Page 43 43
  • Page 44 44
  • Page 45 45
  • Page 46 46
  • Page 47 47
  • Page 48 48
  • Page 49 49
  • Page 50 50
  • Page 51 51
  • Page 52 52
  • Page 53 53
  • Page 54 54
  • Page 55 55
  • Page 56 56
  • Page 57 57
  • Page 58 58
  • Page 59 59
  • Page 60 60
  • Page 61 61
  • Page 62 62
  • Page 63 63
  • Page 64 64
  • Page 65 65
  • Page 66 66
  • Page 67 67
  • Page 68 68
  • Page 69 69
  • Page 70 70
  • Page 71 71
  • Page 72 72
  • Page 73 73
  • Page 74 74
  • Page 75 75
  • Page 76 76
  • Page 77 77
  • Page 78 78
  • Page 79 79
  • Page 80 80
  • Page 81 81
  • Page 82 82
  • Page 83 83
  • Page 84 84
  • Page 85 85
  • Page 86 86
  • Page 87 87
  • Page 88 88
  • Page 89 89
  • Page 90 90
  • Page 91 91
  • Page 92 92
  • Page 93 93
  • Page 94 94
  • Page 95 95
  • Page 96 96
  • Page 97 97
  • Page 98 98
  • Page 99 99
  • Page 100 100
  • Page 101 101
  • Page 102 102
  • Page 103 103
  • Page 104 104
  • Page 105 105
  • Page 106 106
  • Page 107 107
  • Page 108 108
  • Page 109 109
  • Page 110 110
  • Page 111 111
  • Page 112 112
  • Page 113 113
  • Page 114 114
  • Page 115 115
  • Page 116 116
  • Page 117 117
  • Page 118 118
  • Page 119 119
  • Page 120 120
  • Page 121 121
  • Page 122 122
  • Page 123 123
  • Page 124 124
  • Page 125 125
  • Page 126 126
  • Page 127 127
  • Page 128 128
  • Page 129 129
  • Page 130 130
  • Page 131 131
  • Page 132 132
  • Page 133 133

Lovibond 00386455 - MD1x0/200 - Manganese HR PP, Manganese LR PP, Manganese T Manuale utente

Tipo
Manuale utente